HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzenesulfonic acid → HCID 86738432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | Phenylhydrazine | HCID 7516 | — |
| Reactant | 1-(5-Methyl-3-phenylisoxazol-4-yl)ethanone | HCID 318524 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86738432 | HCID 86738432 | — |
Reaction Steps
A mixture of 80.4 g. (0.4 mole) of 4-acetyl-5-methyl-3-phenyl isoxazole, 39.4 ml. (0.4 mole) of phenyl hydrazine and 500 mg. toluenesulfonic acid in 400 ml. ethanol is stirred at room temperature for 48 hours. The resulting solid is filtered and washed with cold ether to give 1-(5-methyl-3-phenyl-4-isoxazolyl)-1-ethanone phenyl hydrazone; m.p. 129°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336378 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-3a157e8ee4ac4209bf319890f75cb5b2 |
| Source note | uspto-grants-1982_06 |