HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20535077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 2-Acetylcyclohexanone | HCID 13400 | — |
| Reactant | HCID 12960442 | HCID 12960442 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20535077 | HCID 20535077 | 9.5% |
Reaction Steps
4-Amino-5-hydrazino-3-mercapto-1,2,3-triazole (7.3 g, 0.05 mol), 7.0 g (0.05 mol) acetyl cyclohexanone, 1.25 ml concentrated hydrochloric acid, and 350 ml ethanol are refluxed for 3 hours, evaporated to dryness, and recrystallized from ethyl acetate to give 1.2 g of white crystals, m.p. 201°-2°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04336375 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-2edbb1fe40f8497a99b74becf493fc76 |
| Source note | uspto-grants-1982_06 |