HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trichloroacetyl chloride → HCID 12851603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trichloroacetyl chloride | HCID 6420 | — |
| Reactant | HCID 13360534 | HCID 13360534 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12851603 | HCID 12851603 | 91% |
Reaction Steps
A solution of 14.7 grams (0.05 mole) 5-anilino-3-trichloromethyl-1,2,4-thiadiazole and 18.0 grams (0.1 mole) trichloroacetyl chloride in 200 milliliters toluene was refluxed at about 110° C. for 20 hours. After removal of the low boiling material in vacuo, the resulting residue was recrystallized from benzene to give 20.0 grams (91% yield) pure product; m.p. 158° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337081 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-e59dcb71c7134e9896703f33c1680479 |
| Source note | uspto-grants-1982_06 |