HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Piperidone → HCID 20469880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Piperidone | HCID 12665 | — |
| Reactant | 6-Chloro-1-hexanol | HCID 74828 | — |
| Product | HCID 20469880 | HCID 20469880 | — |
Reaction Steps
In like manner, 6-chloro-1-hexanol is reacted with 2-piperidone to produce 1-(6-hydroxy-1-hexyl)-2-piperidone. The latter is reacted with methanesulfonyl chloride in methylene chloride in the presence of one equivalent of triethylamine to yield 1-(6-methanesulfonyloxy-1-hexyl)-2-piperidone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337250 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-dbbaa5c2339e47318e0524fdccb5815d |
| Source note | uspto-grants-1982_06 |