HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Chloride → HCID 86738455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Chloride | HCID 5284359 | — |
| Reactant | HCID 23709218 | HCID 23709218 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86738455 | HCID 86738455 | 84.9% |
Reaction Steps
400 mg of calcium chloride in 5 ml of water are added to a solution of 1 g of sodium 2-[4-(3-chlorophenoxy)butyl]oxirane-2-carboxylate in 10 ml of water. The greasy residue which has formed is separated off by decantation, and the sediment is washed by two decantations with little water. The residue is dried over phosphorus pentoxide. 840 mg of the title compound are obtained. Decomposition (without melting) at 225° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337267 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-be105c0303754d5a83be07bbdc85062b |
| Source note | uspto-grants-1982_06 |