Calcium Chloride → HCID 86738455, compound

HRID 1156847Notes

Reaction equation

HRID 1156847 reaction equation
[Cl-].[Ca+2:2].[Cl-].[Cl:4][C:5]1[CH:6]=[C:7]([CH:19]=[CH:20][CH:21]=1)[O:8][CH2:9][CH2:10][CH2:11][CH2:12][C:13]1([C:16]([O-:18])=[O:17])[CH2:15][O:14]1.[Na+]>O>[Cl:4][C:5]1[CH:6]=[C:7]([CH:19]=[CH:20][CH:21]=1)[O:8][CH2:9][CH2:10][CH2:11][CH2:12][C:13]1([C:16]([O-:18])=[O:17])[CH2:15][O:14]1.[Ca+2:2].[Cl:4][C:5]1[CH:6]=[C:7]([CH:19]=[CH:20][CH:21]=1)[O:8][CH2:9][CH2:10][CH2:11][CH2:12][C:13]1([C:16]([O-:18])=[O:17])[CH2:15][O:14]1

Participants

4

Reactant 2

HCID 5284359Calcium ChlorideHCID 23709218HCID 23709218, compound

Product 1

HCID 86738455HCID 86738455, compoundYield 84.9%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

400 mg of calcium chloride in 5 ml of water are added to a solution of 1 g of sodium 2-[4-(3-chlorophenoxy)butyl]oxirane-2-carboxylate in 10 ml of water. The greasy residue which has formed is separated off by decantation, and the sediment is washed by two decantations with little water. The residue is dried over phosphorus pentoxide. 840 mg of the title compound are obtained. Decomposition (without melting) at 225° C.

Workup

  1. customThe greasy residue which has formed
  2. customis separated off by decantation
  3. washthe sediment is washed by two decantations with little water
  4. dry with materialThe residue is dried over phosphorus pentoxide

Sources & evidence

ORD record
ord-be105c0303754d5a83be07bbdc85062b
Source dataset
uspto-grants-1982_06
Patent number
US04337267

Reaction notes

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