4-Toluenesulfonyl chloride → HCID 12917760, compound

HRID 1156959Notes

Reaction equation

HRID 1156959 reaction equation
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH3:12][C:13]1[S:14][C:15]2[CH2:21][CH2:20][CH2:19][CH:18]([CH2:22][OH:23])[C:16]=2[N:17]=1>>[CH3:12][C:13]1[S:14][C:15]2[CH2:21][CH2:20][CH2:19][CH:18]([CH2:22][O:23][S:7]([C:4]3[CH:5]=[CH:6][C:1]([CH3:11])=[CH:2][CH:3]=3)(=[O:9])=[O:8])[C:16]=2[N:17]=1

Participants

3

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 129177484,5,6,7-Tetrahydro-2-methyl-4-benzothiazolemethanol

Product 1

HCID 12917760HCID 12917760, compoundYield 89%

Procedure

This compound is prepared by action of p-toluenesulfonyl chloride on above alcohol (IV), according to the process of Example 1. M.p.=97°-98° C. Yield: 89%.

Sources & evidence

ORD record
ord-be9a0c8b6b7045ceac7d811ad7704546
Source dataset
uspto-grants-1982_06
Patent number
US04337343

Reaction notes

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