HRID1156960

反应详情

EQUATION

反应方程式

HRID 1156960 的结构方程式

REACTANTS

反应物

2

结构：CCOC(=O)C1CCCC(Br)C1=O

Ethyl 3-bromo-2-oxocyclohexane-1-carboxylate

C9H13BrO3

结构：CC(N)=S

Thioacetamide

C2H5NS

PRODUCTS

生成物

1

结构：CCOC(=O)C1CCc2sc(C)nc2C1

Ethyl 2-methyl-4,5,6,7-tetrahydro-1,3-benzothiazole-5-carboxylate

C11H15NO2S

PROCEDURE

实验过程

The compound is prepared by action of thioacetamide on 2-bromo-5-ethoxycarbonyl cyclohexanone (II), as described in Example 1. B.P.0.4 =116°-120° C.

WORKUP

后处理

customB.P.0.4 =116°-120° C.