4-Toluenesulfonyl chloride → HCID 53694437, compound

HRID 1156966Notes

Reaction equation

HRID 1156966 reaction equation
[C:1]1([CH3:11])[CH:6]=[CH:5][C:4]([S:7](Cl)(=[O:9])=[O:8])=[CH:3][CH:2]=1.[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH2:22][CH:21]([CH2:25][OH:26])[C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]>>[CH2:12]([C:16]1[S:17][C:18]2[CH2:24][CH2:23][CH2:22][CH:21]([CH2:25][O:26][S:7]([C:4]3[CH:5]=[CH:6][C:1]([CH3:11])=[CH:2][CH:3]=3)(=[O:9])=[O:8])[C:19]=2[N:20]=1)[CH2:13][CH2:14][CH3:15]

Participants

3

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 12917754HCID 12917754, compound

Product 1

HCID 53694437HCID 53694437, compound

Procedure

The compound is prepared by action of p-toluenesulfonyl chloride on the above derivative (IV), according to the procedure described in Example 1. The product is an undistillable oil which is used crude for the subsequent reactions.

Sources & evidence

ORD record
ord-565bf3e412614e2eb4fbc77017d9eb46
Source dataset
uspto-grants-1982_06
Patent number
US04337343

Reaction notes

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