HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 13023242, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 13023240 | HCID 13023240 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 13023242 | HCID 13023242 | — |
Reaction Steps
Following the procedure set forth in Example 40, 4a-(3-methoxyphenyl)-2-n-pentyl-2,3,4,4a,5,6,7,7a-octahydro-1H-2-pyrindine was reacted with aqueous hydrobromic acid in glacial acetic acid to afford 4a-(3-hydroxyphenyl)-2-n-pentyl-2,3,4,4a,5,6,7,7a-octahydro-1H-2-pyrindine, which was then converted to the corresponding hydrogen bromide salt. M.P. 171°-173° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04337341 |
| Source dataset | uspto-grants-1982_06 |
| ORD ID | ord-31fe6e4ac20541869e351123b95b284c |
| Source note | uspto-grants-1982_06 |