HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178439407, compound → 4-Amino-2-isopropylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178439407 | HCID 178439407 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-Amino-2-isopropylphenol | HCID 586009 | 76% |
Reaction Steps
To a solution of 2-isopropyl-[1,4]benzoquinone 4-oxime (1.1 g, 6.7 mmol) in methanol was added catalytic amount of Ra/Ni complex. The reaction was stirred under 50 psi H2 atmosphere for 5 hrs and filtered through celite. The filtrate was concentrated to give 4-amino-2-isopropyl-phenol (762 mg, 76%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807672B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-cfa465a89aac446dbffa6ded69f5d7d8 |
| Source note | uspto-grants-2010_10 |