HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68695108, compound → HCID 68698459, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68695108 | HCID 68695108 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68698459 | HCID 68698459 | 84.4% |
Reaction Steps
Stir a mixture of 4-methyl-5-nitro-2-pyridin-3-yl-pentan-2-ol (860 mg, 3.84 mmol) and Pt—C(S) (200 mg) in EtOH (25 mL) at room temperature under hydrogen atmosphere (7 atm) for 24 h. Filter through a pad of Celite® and evaporate to obtain 630 mg (84%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807691B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-5819c264c2664d79a296e1d500c00303 |
| Source note | uspto-grants-2010_10 |