HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 11716760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | (3-Bromopropyl)benzene | HCID 12503 | — |
| Reactant | 1-(3-Phenylpropyl)piperidine | HCID 11171707 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11716760 | HCID 11716760 | — |
Reaction Steps
3-Phenylpropylpiperidine (1 eq) was reacted with 3-phenylbromopropane (1 eq) in the presence of K2CO3 in refluxing acetonitrile over night. The product obtained was worked up and purified on a column of silica. The 500 MHz 1H NMR is in accordance with the expected structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807695B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-8f304fe96b774fa197bc0a26ddefe6a3 |
| Source note | uspto-grants-2010_10 |