HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 68618246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Acetonitrile--water (1/1) | HCID 18373917 | — |
| Reactant | HCID 131728368 | HCID 131728368 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68618246 | HCID 68618246 | — |
Reaction Steps
The title compound is prepared as described above for Example 9/step H (Scheme 5) from N-[(3S*,4S*)-4-(tert-butyl-dimethyl-silanyloxymethyl)-pyrrolidin-3-ylmethyl]-N-isobutyl-benzenesulfonamide. MS (LC-MS): 327.1 [M-Boc+H]+; tR (HPLC, Waters Symmetry C18 column, 20-95% CH3CN/H2O/3.5 min, 95% CH3CN/H2O, 2 min, CH3CN and H2O containing 0.1% TFA, flow: 0.6 mL/min): 4.17 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07807709B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-ade3ecd5e70c49368df0c295dc20c982 |
| Source note | uspto-grants-2010_10 |