Ammonia → 3,4-Dihydro-2H-1-benzopyran-4-amine

참여 물질

역할	이름	HCID	투입량
반응물	Ammonia	HCID 222	—
반응물	Chroman-4-one O-methyl-oxime	HCID 54035320	—
반응물	(4E)-N-Methoxy-6-methyl-3,4-dihydro-2H-1-benzopyran-4-imine	HCID 86605441	—
생성물	3,4-Dihydro-2H-1-benzopyran-4-amine	HCID 4961957	—

반응 단계

The title compound was prepared using the procedure as described in Example 7B, substituting the product of Example 16A for the product of Example 7A. 1H NMR (300 MHz, DMSO-d6) δ ppm 7.32 (dd, J 1.0 and 7.5 Hz, 1H), 7. 05 (m, 1H), 6.81 (m, 1H), 6.70 (dd, J 1.0 and 7.5 Hz, 1H), 4.27-4.08 (m, 2H), 3.83 (t, J 6.0 Hz, 1H), 2.03-1.66 (m, 4H). MS (DCI/NH3) m/e 150 (M+H)+.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US07812019B2
출처 데이터셋	uspto-grants-2010_10
ORD ID	ord-36455fce63114ce58a8e230d7d86b904
출처 메모	uspto-grants-2010_10