HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178425624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 6-Methoxy-3,3-dimethyl-2,3,4,5-tetrahydropyridine | HCID 21941393 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178425624 | HCID 178425624 | — |
Reaction Steps
The mixture of 3,3-dimethyl-6-methoxy-2,3,4,5-tetrahydropyridine (9.0 g, 64 mmol) and ammonium chloride (3.4 g, 64 mmol) in dry ethanol (160 mL) was heated to reflux for 2 h. The reaction mixture was then concentrated under reduced pressure and the titled compound was obtained as a white solid (9.9 g, 94.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812014B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-2f0c9aec9ca847ee9650f575ea16b359 |
| Source note | uspto-grants-2010_10 |