HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Desoxypyridoxine hydrochloride → HCID 68644250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Desoxypyridoxine hydrochloride | HCID 67417 | — |
| Reactant | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| Product | HCID 68644250 | HCID 68644250 | 80.3% |
Reaction Steps
The coupling of 4-deoxypyridoxine hydrochloride (5.0 g, 0.026 mol) and α-bromo-p-tolunitrile (5.2 g, 0.026 mol), as described in Example 3, gave 4-(5-hydroxymethyl-2,4-dimethyl-pyridin-3-yloxymethyl)-benzonitrile (22) (5.6 g, 80% yield) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812037B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-024099c7767b4ea798a0636a1b9f4b86 |
| Source note | uspto-grants-2010_10 |