HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Desoxypyridoxine hydrochloride → HCID 58636777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Desoxypyridoxine hydrochloride | HCID 67417 | — |
| Reactant | 3-Iodobenzonitrile | HCID 144341 | — |
| Product | HCID 58636777 | HCID 58636777 | 7.5% |
Reaction Steps
The coupling of 4-deoxypyridoxine hydrochloride (5.6 g, 29.5 mmol) and 3-iodobenzonitrile (10.0 g, 43.0 mmol), as described in Example 81, gave 3-(5-hydroxymethyl-2,4-dimethyl-pyridin-3-yloxy)-benzonitrile (93) (0.5 g, 7.5% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812037B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-127dd101f0604ff29d350c172ace2fc0 |
| Source note | uspto-grants-2010_10 |