HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68445147, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 68443656 | HCID 68443656 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68445147 | HCID 68445147 | — |
Reaction Steps
A mixture of acetic acid 6-trifluoromethyl-benzofuran-3-yl ester (15 g), methanol (100 ml), water (53.8 ml) and 1 N HCl (18.8 ml) was heated at reflux for 6 hrs. Mixture was cooled to room temperature. Crude product was evaporated in vacuo and purified by chromatography to give product 6a (Hexane:EA=18:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07812177B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-f8e148b6579b46eb87406bfd05dac2e3 |
| Source note | uspto-grants-2010_10 |