Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl formate → N'-(4-Bromophenyl)formohydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl formate | HCID 7865 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Bromophenylhydrazine hydrochloride | HCID 12157 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | N'-(4-Bromophenyl)formohydrazide | HCID 13725233 | — |
반응 단계
10 g of 4-bromophenylhydrazine hydrochloride are dissolved in 30 ml of water; 6.2 g of K2CO3 and 36 ml of methyl formate are added and then the mixture is heated at reflux for 1 hour and then at AT for 12 hours. The precipitate formed is filtered off and then washed with an isopropanol/PE mixture (50/50; v/v). This gives 10.5 g of the expected compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07812165B2 |
| 출처 데이터셋 | uspto-grants-2010_10 |
| ORD ID | ord-7d3c43a5e55240858f88758845a1dab7 |
| 출처 메모 | uspto-grants-2010_10 |