HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1160382Generated: November 2, 2026
HCID 68690984, compound → HCID 68688085, compound
https://huagongshe.com/reaction/1160382
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 68690984 | HCID 68690984 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68688085 | HCID 68688085 | — |
Reaction Steps
46.6 g (0.023 M) of methyl 2-(4-hydroxybut-1-ynyl)benzoate and 5 g of wet 10% palladium-on-charcoal are added to 900 ml of methanol in a 2000 ml stainless-steel autoclave. The reaction medium is then stirred under hydrogen pressure (10 bar) at 70° C. for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07816397B2 |
|---|
| Source dataset | uspto-grants-2010_10 |
|---|
| ORD ID | ord-e42e3f00014a415cb9458d0b8e5407e0 |
|---|
| Source note | uspto-grants-2010_10 |
|---|
