HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylcyclohexylamine → HCID 11739881, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylcyclohexylamine | HCID 7514 | — |
| Reactant | 1-(4-CHLOROPHENYL)-5-PROPYL-1H-PYRAZOLE-4-CARBONYL CHLORIDE | HCID 2777585 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11739881 | HCID 11739881 | — |
Reaction Steps
To a suspension of 1-(4-chlorophenyl)-5-propyl-pyrazole-4-carbonyl chloride (commercially available, 302 mg, 1.07 mmol) in DCM (5 ml) was added 1 drop of DMF followed by N-methylcyclohexylamine (349 μL, 2.68 mmol). The reaction mixture was stiffed at room temperature for two hours then stopped.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07816391B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-6db79471ccfc40f6a761b5afc1430ec3 |
| Source note | uspto-grants-2010_10 |