Methyl 4-Formylbenzoate → 4-(1-Hydroxy-heptyl)-benzoic acid methyl ester

HRID 1160854Notes

Reaction equation

HRID 1160854 reaction equation
[CH3:1][O:2][C:3](=[O:12])[C:4]1[CH:9]=[CH:8][C:7]([CH:10]=[O:11])=[CH:6][CH:5]=1.[CH2:13]([Mg]Cl)[CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]>>[CH3:1][O:2][C:3](=[O:12])[C:4]1[CH:9]=[CH:8][C:7]([CH:10]([OH:11])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18])=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 15294Methyl 4-FormylbenzoateHCID 178444611HCID 178444611, compound

Product 1

HCID 595181434-(1-Hydroxy-heptyl)-benzoic acid methyl ester

Procedure

This compound is made from 4-formyl-benzoic acid methyl ester and n-hexylmagnesium chloride following the general method of Preparation 1.

Workup

  1. customthe general method of Preparation 1

Sources & evidence

ORD record
ord-aeb2b0cea09a4a6a90eab4af9069b0c8
Source dataset
uspto-grants-2010_10
Patent number
US07816557B2

Reaction notes

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