Methanol → HCID 59515704, compound

Participants

Reaction Steps

A mixture of (R)-2-(6-methoxy-5-nitro-1-oxoisoquinolin-2(1H)-yl)propanamide (200 mg, 0.0007 mol), methanol (20 mL, 0.5 mol) and palladium, 10% weight on charcoal (21 mg, 0.00017 mol) was stirred under hydrogen (1 atm) for 3 h. The reaction mixture was filtered over celite and the solvent removed to obtain the product as a brown solid. MS m/z=263.3 (M+H).

Provenance & Evidence