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HRID1161326

反应详情

EQUATION

反应方程式

HRID 1161326 的结构方程式

REACTANTS

反应物

4
结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：Clc1ccc(-c2nc3ccccc3[nH]2)cc1
HCID759417

2-(4-Chlorophenyl)benzimidazole

C13H9ClN2

结构：CCOC(=O)C(Br)C1CCCCC1
HCID2762757

ethyl 2-bromo-2-cyclohexylacetate

C10H17BrO2

结构：O=C(O)c1ccc(NC(=O)C(C2CCCCC2)n2c(-c3ccc(Cl)nc3)nc3cc(F)c(F)cc32)c(Cl)c1
HCID44197691

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(C1CCCCC1)n1c(-c2ccc(Cl)cc2)nc2ccccc21
HCID66619211

Ethyl 2-(4-chlorophenyl)-α-cyclohexyl-1H-benzimidazole-1-acetate

C23H25ClN2O2

收率 58%

PROCEDURE

实验过程

This compound was synthesized in analogy to example 22, intermediate b, from 2-(4-chloro-phenyl)-1H-benzoimidazole (commercially available), bromo-cyclohexyl-acetic acid ethyl ester (commercially available) and cesium carbonate, to provide the final compound as a colorless solid (58%).