HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methylthio)aniline → (2,6-Diphenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methylthio)aniline | HCID 66038 | — |
| Reactant | 4-Chloro-2,6-diphenylpyrimidine | HCID 582041 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | (2,6-Diphenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine | HCID 58626107 | — |
Reaction Steps
4-Chloro-2,6-diphenyl-pyrimidine (0.4 g, 1.5 mmol) was reacted with 4-methylsulfanyl-phenylamine (0.22 g, 1.6 mmol) in a solvent n-butanol (10 mL) at reflux temperature for 12 hours to yield (2,6-diphenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-c17725e9f24e47b3a2331d7d3e489e4b |
| Source note | uspto-grants-2010_10 |