HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propan-2-one--water (1/1) → (2,6-Diphenyl-pyrimidin-4-yl)-(4-methanesulfonyl-phenyl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propan-2-one--water (1/1) | HCID 18366337 | — |
| Reactant | Potassium hydroxy sulfite | HCID 23707502 | — |
| Reactant | (2,6-Diphenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine | HCID 58626107 | — |
| Product | (2,6-Diphenyl-pyrimidin-4-yl)-(4-methanesulfonyl-phenyl)-amine | HCID 58626171 | — |
Reaction Steps
(2,6-Diphenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine (0.17 g, 0.46 mmol) was oxidized with oxone (0.84 g, 1.3 mmol) in acetone-water (2:1, 9 mL) at room temperature for 5 minutes. Solid was filtered and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-02c2c8a6ef704c328a7a089bebd0bdfd |
| Source note | uspto-grants-2010_10 |