HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propan-2-one--water (1/1) → HCID 58626100, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propan-2-one--water (1/1) | HCID 18366337 | — |
| Reactant | Potassium hydroxy sulfite | HCID 23707502 | — |
| Reactant | HCID 58626075 | HCID 58626075 | — |
| Product | HCID 58626100 | HCID 58626100 | — |
Reaction Steps
(6-Chloro-2-phenyl-pyrimidin-4-yl)-(4-methylsulfanyl-phenyl)-amine (1 g, 3.03 mmol) was treated with oxone in acetone-water at temperature in the range of 20-40° C. for 1 hour to yield the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-0ec23fb2f709411395142421ac37e96c |
| Source note | uspto-grants-2010_10 |