HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidin-4-ol → HCID 58626140, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | HCID 58626100 | HCID 58626100 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 58626140 | HCID 58626140 | — |
Reaction Steps
The (6-chloro-2-phenyl-pyrimidin-4-yl)-(4-methanesulfonyl-phenyl)-amine (0.18 g, 0.48 mmol) was treated with 4-hydroxy piperidine (0.097 g, 0.97 mmol) in n-butanol at refluxing temperature for 12 hour to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-7e535f392d164d9ba33c615322234efd |
| Source note | uspto-grants-2010_10 |