HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 58626077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,4,6-Trichloropyrimidine | HCID 77378 | — |
| Reactant | 4-(Trifluoromethoxy)aniline | HCID 600848 | — |
| Solvent | Chloroform hexane | HCID 21585165 | — |
| Product | HCID 58626077 | HCID 58626077 | — |
Reaction Steps
The title compound was prepared by reacting 2,4,6-trichloro pyrimidine (2 g, 10 mmol) with 4-trifluoromethoxy aniline (1.94 g, 10 mmol) in presence of triethylamine (5.5 g, 50 mmol) in a solvent chloroform: hexane (1:1, 20 mL) at reflux temperature for 7 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-85f973c2e907434188d3267a987b1834 |
| Source note | uspto-grants-2010_10 |