HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 58626073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 58626111 | HCID 58626111 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 58626073 | HCID 58626073 | — |
Reaction Steps
[4-Chloro-6-(3-methanesulfonyl-phenyl)-pyrimidin-2-yl]-(4-trifluoromethoxy-phenyl)-amine (0.14 g, 0.3 mmol) was reacted with morpholine (0.09 mL) in a solvent n-butanol (7 mL) at reflux temperature for 12 hours. Solid was filtered and dried to afford the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820654B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-68e1c68e7051499084111d69bcc8e80a |
| Source note | uspto-grants-2010_10 |