HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 17961828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | N-methylhydroxylamine hydrochloride | HCID 77906 | — |
| Reactant | HCID 17961855 | HCID 17961855 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17961828 | HCID 17961828 | — |
Reaction Steps
1-Benzyloxycarbonyl-2-cyanoindoline was added to a solution of triethylamine (2 eq.) and MeNHOH.HCl (2 eq.) in EtOH. After stirring overnight the reaction mixture was evaporated, dissolved in EtOAc, washed with water, dried over Na2SO4 and evaporated to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820660B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-b3f1a868bb7f421aa38c158dad9eaa81 |
| Source note | uspto-grants-2010_10 |