HCID 178499103, compound → HCID 178499119, compound

HRID 1161894Notes

Reaction equation

HRID 1161894 reaction equation
[OH:1][C:2]1[C:7]([OH:8])=[C:6]([C:9]([O:11][CH3:12])=[O:10])[N:5]=[C:4](C(O)=O)[N:3]=1>Cl>[OH:8][C:7]1[C:6]([C:9]([O:11][CH3:12])=[O:10])=[N:5][CH:4]=[N:3][C:2]=1[OH:1]

Participants

3

Reactant 1

HCID 178499103HCID 178499103, compound

Product 1

HCID 178499119HCID 178499119, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Procedure

A solution of the product of Step 1 in HCl 1N solution was stirred for 6 hours at 90° C. Reaction mixture was filtered and the solid washed with HCl 1N. Evaporation of the filtrate afforded the title product as a solid.

Workup

  1. customReaction mixture
  2. filtrationwas filtered
  3. washthe solid washed with HCl 1N
  4. customEvaporation of the filtrate

Sources & evidence

ORD record
ord-18b22348435a47278c4ea31efccbde95
Source dataset
uspto-grants-2010_10
Patent number
US07820660B2

Reaction notes

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