HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 66893075, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 66894542 | HCID 66894542 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66893075 | HCID 66893075 | — |
Reaction Steps
Oxalyl chloride (0.1 mL, 1.1 mmol) was dissolved in dry DCM (2 mL) and DMF (0.9 mL, 1.1 mmol) was added (very exothermic reaction). {5-[(2-Methoxy-5-methylphenyl)sulfonyl]-1-benzofuran-7-yl}methanol (370 mg, 1.1 mmol; Intermediate 68)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820675B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-45b8089de67243c1a4f7ada2cb137fe1 |
| Source note | uspto-grants-2010_10 |