HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonic Acid → HCID 66892329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonic Acid | HCID 7371 | — |
| Reactant | Methyl 2,3-dihydrobenzofuran-7-carboxylate | HCID 15062252 | — |
| Reactant | HCID 66893378 | HCID 66893378 | — |
| Product | HCID 66892329 | HCID 66892329 | — |
Reaction Steps
The title compound was prepared according to the procedure of Intermediate 66 starting from methyl 2,3-dihydro-1-benzofuran-7-carboxylate (1 g, 5.6 mmol; Intermediate 65) and benzenesulfonic acid (0.89 g, 5.6 mmol). Yield: 882 mg (49%). MS (ESI+) for C16H14O5S m/z 319 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820675B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-fee4e1cac5f94de897e8e497b8d06073 |
| Source note | uspto-grants-2010_10 |