HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66892329, compound → HCID 66892653, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66892329 | HCID 66892329 | — |
| Reactant | HCID 66893431 | HCID 66893431 | — |
| Product | HCID 66892653 | HCID 66892653 | — |
Reaction Steps
The title compound was prepared according to the procedure of Intermediate 67 starting from methyl 5-(phenylsulfonyl)-2,3-dihydro-1-benzofuran-7-carboxylate (198 mg, 0.6 mmol; obtained in Step 1). Yield: 80 mg (41%) after purification by preparative HPLC (System F; 40-70% MeCN). MS (ESI+) for C16H14O5S m/z 317 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820675B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-6448a83ad50444f588ae493829dc4139 |
| Source note | uspto-grants-2010_10 |