HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66893263, compound → HCID 66891956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66893263 | HCID 66893263 | — |
| Reactant | HCID 66893431 | HCID 66893431 | — |
| Product | HCID 66891956 | HCID 66891956 | — |
Reaction Steps
The title compound was prepared according to the procedure of Intermediate 67 starting from methyl 5-[(4-methylphenyl)sulfonyl]-2,3-dihydro-1-benzofuran-7-carboxylate (117 mg, 0.4 mmol; obtained in Step 1). Yield: 62 mg (53%) after purification by preparative HPLC (System F; 40-60% MeCN). MS (ESI+) for C17H16O5S m/z 331 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820675B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-04de6e1739f24c67893cb1c907c8c1de |
| Source note | uspto-grants-2010_10 |