HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl bromoacetate → HCID 68647969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl bromoacetate | HCID 79177 | — |
| Reactant | HCID 68648279 | HCID 68648279 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68647969 | HCID 68647969 | — |
Reaction Steps
{[2-(4-Isopropyl-phenyl)-pyrimidin-4-yl]-thiophen-2-ylmethyl-amino}-acetic acid tert-butyl ester was prepared (149 mg) from [2-(4-isopropyl-phenyl)-pyrimidin-4-yl]-thiophen-2-ylmethyl-amine (135 mg, 0.44 mmol) and bromoacetic acid tert-butyl ester in THF by following the general procedure F. LCMS m/z: 425 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820704B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-e1f4118df3b348eab9ccbf728d2a646b |
| Source note | uspto-grants-2010_10 |