HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Chloride → HCID 178438899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 68647686 | HCID 68647686 | — |
| Product | HCID 178438899 | HCID 178438899 | 4.1% |
Reaction Steps
[4-(4-Isopropyl-phenyl)-thiazol-2-yl]-[2-(1H-tetrazol-5-yl)-benzyl]-thiophen-2-ylmethyl-amine (6.0 mg) was prepared following general procedure H from the corresponding nitrile (130 mg, 0.31 mmol), ammonium chloride (3.1 mmol) and sodium azide (3.1 mmol). Purification (Silica gel, methanol/DCM 3:97) provided the product. LCMS m/z: 474 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820704B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-65975b5577b44a2e9fca50e8be615911 |
| Source note | uspto-grants-2010_10 |