HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 86079799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | methyl 1H-indazole-3-carboxylate | HCID 657476 | — |
| Reactant | Fmoc isothiocyanate | HCID 4154759 | — |
| Product | HCID 86079799 | HCID 86079799 | — |
Reaction Steps
1-Thiocarbamoyl-1H-indazole-3-carboxylic acid methyl ester was prepared (113 mg) following general procedure D using 1H-Indazole-3-carboxylic acid methyl ester (120 mg, 0.69 mmol), Fmoc isothiocyanate (213 mg, 0.76 mmol), and diethyl amine (0.5 mL). LCMS m/z: 236 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820704B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-2528cafedf634f978fd6c539511c87c6 |
| Source note | uspto-grants-2010_10 |