HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminocyclohexanecarboxylate → HCID 86601765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminocyclohexanecarboxylate | HCID 422580 | — |
| Reactant | Fmoc isothiocyanate | HCID 4154759 | — |
| Product | HCID 86601765 | HCID 86601765 | 26.7% |
Reaction Steps
4-Thioureido-cyclohexanecarboxylic acid methyl ester (150 mg) compound was prepared following general procedure D using 4-Amino-cyclohexanecarboxylic acid methyl ester (500 mg, 11.0 mmol), and Fmoc-isothiocyanate (730 mg). Purification: (Silica gel, ethyl acetate/hexane 1:1). LCMS m/z: 217.0 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820704B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-3e6f3d02870c49e1bb2a9e6d6506e51e |
| Source note | uspto-grants-2010_10 |