HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-1-benzofuran-2-carboxylic acid → HCID 58748253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-1-benzofuran-2-carboxylic acid | HCID 937838 | — |
| Reactant | tert-Butyl (3R)-3-(aminomethyl)pyrrolidine-1-carboxylate | HCID 1515152 | — |
| Product | HCID 58748253 | HCID 58748253 | — |
Reaction Steps
67.1 Using general procedure E, (R)-3-aminomethyl-1-N-tert-butoxycarbonyl-pyrrolidine was coupled with 5-chloro-benzofuran-2-carboxylic acid to give (R)-3-{[(5-chloro-benzofuran-2-carbonyl)-amino]-methyl}-pyrrolidine-1-carboxylic acid tert-butyl ester. White solid. MS377.3 ([M−H]−)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820699B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-eea213876f3a4a37a2128f9118ffd1b3 |
| Source note | uspto-grants-2010_10 |