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HRID1163393

反应详情

EQUATION

反应方程式

HRID 1163393 的结构方程式

REACTANTS

反应物

2
结构：CCc1cccc(CC)c1N=C=S
HCID141193

2,6-Diethylphenyl isothiocyanate

C11H13NS

结构：CC(C)n1ccnc1Nc1nc2ccc(C(=O)Nc3ccc4cn[nH]c4c3)cc2[nH]1
HCID59522617

未命名化合物

PRODUCTS

生成物

1
结构：CCc1cccc(CC)c1Nc1nc2ccc(C(=O)Nc3ccc4cn[nH]c4c3)cc2[nH]1
HCID58970720

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1.CN(C)C=O
溶剂HCID21974620

未命名化合物

PROCEDURE

实验过程

A solution of 1,3-diethyl-2-isothiocyanatobenzene (0.5 mmol) in 1:1 DMF/THF (2 mL) was reacted with 3,4-diamino-N-(1H-indazol-6-yl)-benzamide (0.5 mmol; see Example 25) according to general procedure B to yield 2-(2,6-diethylphenylamino)-3H-benzimidazole-5-carboxylic acid (1H-indazol-6-yl)-amide. MS: m/z 425 (M+H)+.