HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 68446679, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Ammonium Hydroxide | HCID 14923 | — |
| Reactant | HCID 68444790 | HCID 68444790 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 68446679 | HCID 68446679 | — |
Reaction Steps
A solution of the aforementioned amide (3 mmol) in dioxane was reacted with aqueous NH4OH and subsequently with diethylamine using the one-pot procedure described for Example 115 to yield 4-amino-N-benzothiazol-6-yl-2-diethylamino-5-nitrobenzamide as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820821B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-a92af592b00f42159c4f89afcceacf21 |
| Source note | uspto-grants-2010_10 |