HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178426306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178426307 | HCID 178426307 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178426306 | HCID 178426306 | — |
Reaction Steps
The product from Example 157 was treated with 4M HCl in dioxane employing the procedure described for Example 156 to afford 6-(4-Aminopiperidin-1-yl)-2-(3-methylpyridin-2-ylamino)-1H-benzimidazole-5-carboxylic acid (1H-indazol-6-yl)-amide as a hydrochloride salt. MS: m/z 521 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820821B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-939a7a91b8bb4acd88321a10ef09664a |
| Source note | uspto-grants-2010_10 |