HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178506142, compound → HCID 178506143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178506142 | HCID 178506142 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178506143 | HCID 178506143 | — |
Reaction Steps
A solution of [5-(1H-Indazol-6-ylethynyl)-1H-benzoimidazol-2-yl]-(2-trifluoromethylphenyl)-amine (0.3 mmol; see Example 159) in ethanol (3 mL) was reduced under hydrogenation conditions at 50 psi as described in general procedure to yield {5-[2-(1H-indazol-6-yl)-ethyl]-1H-benzimidazol-2-yl}-(2-trifluoromethylphenyl)amine. MS: m/z 422 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07820821B2 |
| Source dataset | uspto-grants-2010_10 |
| ORD ID | ord-617548b1056e4cb283e131159bd120a8 |
| Source note | uspto-grants-2010_10 |