Dichloromethane → Tert-butyl 3-(methanesulfonyloxy)azetidine-1-carboxylate

HRID 116349Notes

Reaction equation

HRID 116349 reaction equation
[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([OH:12])[CH2:11]1.[CH2:25]([Cl:26])[Cl:27].[CH3:13][S:14]([Cl:15])(=[O:16])=[O:17].[CH3:18][CH2:19][N:20]([CH2:21][CH3:22])[CH2:23][CH3:24]>>[C:1]([CH3:2])([CH3:3])([CH3:4])[O:5][C:6](=[O:7])[N:8]1[CH2:9][CH:10]([O:12][S:14]([CH3:13])(=[O:16])=[O:17])[CH2:11]1

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 8471TriethylamineHCID 31297Methanesulfonyl chlorideHCID 2756801Tert-butyl 3-hydroxyazetidine-1-carboxylate

Product 1

HCID 10753243Tert-butyl 3-(methanesulfonyloxy)azetidine-1-carboxylate

Sources & evidence

ORD record
ord-31b0849cdf3c44169510b5f89c0f913e
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (2/10)

Reaction notes

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