HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 54315930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | 2-Methoxy-1-Pyrroline | HCID 353443 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | HCID 54315930 | HCID 54315930 | 7.1% |
Reaction Steps
According to HU-Patent Specification No. 167 676 2-methoxy-1-pyrroline is heated with diethyl-ethoxymethylene-malonate for 8 hours in the presence of ammonium acetate and the reaction mixture is processed in a complicated manner to give ethyl 4-oxo-4,6,7,8-tetrahydro-pyrrolo[1,2-a]pyrimidine with a yield of 7.1%. No melting point of the product is given, the product is characterized only by IR and PMR spectra.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367229 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-9e324a26c9254c95b33828ac5f9a3824 |
| Source note | uspto-grants-1983_01 |