HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 20438507, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 12778914 | HCID 12778914 | — |
| Product | HCID 20438507 | HCID 20438507 | 77.5% |
Reaction Steps
2.08 g. of ethyl 4-oxo-4,6,7,8-tetrahydro-pyrrolo[1,2-a]pyrimidine-3-carboxylate is added to 10 ml. of 98% by weight of hydrazine hydrate and the mixture is allowed to stand for 1 hour at room temperature and the obtained crystals are filtered and washed with water. 1.5 g. (77.5%) of 4-oxo-4,6,7,8-tetrahydro-pyrrolo(1,2-a)pyrimidine-3-carbohydrazide is obtained, melting at 180°-181° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367229 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-2c9ea199fd2b4ce1b9d36480cfc4655b |
| Source note | uspto-grants-1983_01 |