Hydrochloric Acid → HCID 13091964, compound

HRID 1163917Notes

Reaction equation

HRID 1163917 reaction equation
[Cl:1][C:2]1C=CC=C[C:3]=1C(O[Si](C)(C)C)C#N.Cl.Cl.[Cl:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[CH:25]([OH:29])[C:26](=[NH:28])[OH:27]>>[ClH:1].[Cl:18][C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][C:20]=1[CH:25]([OH:29])[C:26](=[NH:28])[O:27][CH2:2][CH3:3]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 11413764HCID 11413764, compoundHCID 178479560HCID 178479560, compound

Product 1

HCID 13091964HCID 13091964, compound

Procedure

By the procedure of Example 2, 2-(2-chlorophenyl)-2-trimethylsiloxyethanenitrile (15 g.) in 375 l. of saturated ethanolic hydrogen chloride was converted to ethyl 1-(2-chlorophenyl-1-hydroxymethanecarboximidate hydrochloride [13.4 g., 85%; m.p. 127°-129° C. (dec); ir (KBr) 3125, 3003, 2899, 1653, 1531 cm-1 ].

Sources & evidence

ORD record
ord-fc1eea7474404a0c899b479da4c8e909
Source dataset
uspto-grants-1983_01
Patent number
US04367234

Reaction notes

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